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On the Construction of a Calibration Curve Using a Glow Discharge Emission Spectrometer for Measuring the Hydrogen Content in Zirconium Alloys ; К вопросу о построении калибровочной кривой с помощью спектрометра эмиссионного тлеющего разряда для измерений содержания водорода в сплавах циркония

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اقرأ أكثر حفظ في قائمتي
  • معلومة اضافية
    • Contributors:
      The work was supported by the State Assignment «Science» within the framework of the scientific project No. FSWW-2023–0005.; Работа выполнена при финансовой поддержке Государственного задания «Наука» в рамках научного проекта № FSWW-2023–0005.
    • بيانات النشر:
      Ural Research Institute of Metrology
    • الموضوع:
      2024
    • Collection:
      Reference materials (E-Journal) / Стандартные образцы
    • نبذة مختصرة :
      One of the main directions of modern activity of metrology researchers is to provide the real sector of the economy of the Russian Federation with reference materials that have no analogues in the country. The article discusses the research of highly efficient materials for fuel cladding (fuel elements) in the active zones of thermal reactors, the scope of which is wide. The purpose of the study is the development of samples of the composition of the zirconium alloy to establish and control the stability of the calibration curves of spectrometers when determining the mass fraction of hydrogen, provided that the metrological and technical characteristics of the reference material meet the requirements of the measurement procedure. The main methods for determining the hydrogen content in materials are analyzed. It has been established that the method of glow discharge optical emission spectroscopy has found the widest application. It has also been established that zirconium alloys are chosen as the main material in most cases.The need to create samples for constructing a calibration curve for spectrometers for measuring the hydrogen content in a zirconium alloy is noted. Samples of zirconium alloy Zr-1Nb (grade Э110) have been developed to construct a calibration curve using a glow discharge emission spectrometer for measurements with a mass fraction of hydrogen from 0.034 to 0.498 %. Calibration is carried out using the developed samples to obtain a calibration curve using the example of an emission glow discharge spectrometer of the GD Profiler2 type. The relative error of the hydrogen mass fraction obtained during calibration does not exceed ± 10 %.The practical significance of the study lies in the development of samples that can be used to calibrate spectrometers based on the method of glow discharge optical emission spectroscopy. ; Одно из магистральных направлений современной деятельности исследователей-метрологов – обеспечение реального сектора экономики Российской Федерации стандартными образцами, аналоги ...
    • File Description:
      application/pdf
    • Relation:
      https://www.rmjournal.ru/jour/article/view/477/329; Puls M. P. The effect of hydrogen and hydrides on the integrity of zirconium alloy components: delayed hydride cracking. London: Springer, 2012. 452 p. https://doi.org/10.1007/978-1-4471-4195-2; Positron annihilation spectroscopy study of defects in hydrogen loaded Zr-1Nb alloy / J. Bordulev [et al.] // Journal of Alloys and Compounds. 2019. Vol. 798. P. 685–694. https://doi.org/10.1016/j.jallcom.2019.05.186; Microstructure and hydride embrittlement of zirconium model alloys containing niobium and tin / S. J. Oh [et al.] // Materials Science and Engineering. 2011. Vol. 528. Iss. 10. P. 3771–3776. https://doi.org/10.1016/j.msea.2011.01.093; On the role of hydrogen filled vacancies on the embrittlement of zirconium: An ab initio investigation / P. A. T. Olsson [et al.] // Journal of Nuclear Materials. 2015. Vol. 467. Part 1. P. 311–319. https://doi.org/10.1016/j.jnucmat.2015.09.056; Northwood D. O., Kosasih U. Hydrides and delayed hydrogen cracking in zirconium and its alloys // International Metals Reviews. 1983. Vol. 28. Iss. 1. P. 92–121. https://doi.org/10.1179/imtr.1983.28.1.92; Hydrogen interactions with defects in crystalline solids / S. M. Myers [et al.] // Reviews of Modern Physics. 1992. Vol. 64. Iss. 2. P. 559–617. https://doi.org/10.1103/RevModPhys.64.559; Hydrogen and vacancy clustering in zirconium / C. Varvenne [et al.] // Acta Materialia. 2015. Vol. 102. P. 56–69. https://doi.org/10.1016/j.actamat.2015.09.019; Investigation of hydrogen distribution from the surface to the depth in technically pure titanium alloy with the help of glow discharge optical emission spectroscopy / A. M. Lider [et al.] // Applied Mechanics and Materials. 2013. Vol. 302. P. 92–96. https://doi.org/10.4028/www.scientific.net/AMM.302.92; Quantitative depth profile analysis of metallic coatings by pulsed radiofrequency glow discharge optical emission spectrometry / P. Sánchez [et al.] // Analytica chimica acta. 2011. Vol. 684. Iss. 1. P. 47–53. https://doi.org/10.1016/j.aca.2010.10.039; Glow discharge optical emission spectroscopy: A practical guide / R. Payling [et al.]. Cambridge (UK): RSC Analytical Spectroscopy Monographs, 2003. https://doi.org/10.1039/9781847550989; Marcus R. K., Broekaert J. A. C. Glow discharge plasmas in analytical spectroscopy // TrAC Trends in Analytical Chemistry. 2003. Vol. 22, Iss. 3. P. 186 https://doi.org/10.1016/S0165-9936(03)00307-8; Kudiiarov V. N., Lider A. M., Harchenko S. Y. Hydrogen accumulation in technically pure titanium alloy at saturation from gas atmosphere // Advanced Materials Research. 2014. Vol. 880. P. 68–73. https://doi.org/10.4028/www.scientific.net/AMR.880.68; Andreasen A. Design and building of a new experimental setup for testing hydrogen storage materials // Risø-Report. 2005. P. 52. https://doi.org/10.13140/RG.2.2.32450.99527; Checchetto R., Trettel G., Miotello A. Sievert-type apparatus for the study of hydrogen storage in solids // Measurement Science and Technology. 2003. Vol. 15. Iss. 1. P. 127–130. DOI:10.1088/0957–0233/15/1/017; https://www.rmjournal.ru/jour/article/view/477
    • الرقم المعرف:
      10.20915/2077-1177-2024-20-1-85-92
    • Rights:
      Authors who publish with this journal agree to the following terms:Authors retain copyright and grant the journal right of first publication with the work simultaneously licensed under a Creative Commons Attribution License that allows others to share the work with an acknowledgement of the work's authorship and initial publication in this journal.Authors are able to enter into separate, additional contractual arrangements for the non-exclusive distribution of the journal's published version of the work (e.g., post it to an institutional repository or publish it in a book), with an acknowledgement of its initial publication in this journal.Authors are permitted and encouraged to post their work online (e.g., in institutional repositories or on their website) prior to and during the submission process, as it can lead to productive exchanges, as well as earlier and greater citation of published work (See The Effect of Open Access). ; Авторы, публикующие в данном журнале, соглашаются со следующим:Авторы сохраняют за собой авторские права на работу и предоставляют журналу право первой публикации работы на условиях лицензии Creative Commons Attribution License, которая позволяет другим распространять данную работу с обязательным сохранением ссылок на авторов оригинальной работы и оригинальную публикацию в этом журнале.Авторы сохраняют право заключать отдельные контрактные договорённости, касающиеся не-эксклюзивного распространения версии работы в опубликованном здесь виде (например, размещение ее в институтском хранилище, публикацию в книге), со ссылкой на ее оригинальную публикацию в этом журнале.Авторы имеют право размещать их работу в сети Интернет (например в институтском хранилище или персональном сайте) до и во время процесса рассмотрения ее данным журналом, так как это может привести к продуктивному обсуждению и большему количеству ссылок на данную работу (См. The Effect of Open Access).
    • الرقم المعرف:
      edsbas.C57F751F