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Characterization of adherence for Ti6Al4V films RF magnetron sputter grown on stainless steels ; Caracterización de la adherencia para películas de Ti6Al4V depositadas por medio de pulverización catódica magnetrón RF sobre acero inoxidable

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  • معلومة اضافية
    • بيانات النشر:
      Universidad Nacional de Colombia - Sede Medellín - Facultad de Minas
    • الموضوع:
      2014
    • Collection:
      Universidad Nacional de Colombia: Portal de Revistas UN
    • نبذة مختصرة :
      Ti6Al4V films were grown on UNS S31600 austenitic stainless steel samples by RF magnetron sputtering. On top of samples, macroindentation tests were carried out to characterize the film to substrate adherence according to the recommended VDI 3198 procedure. Sputter deposition experiments varying both chamber pressure and target applied power were carried out. All films displayed superior adhesion to the substrates. A non-monotonic relationship between adherence and chamber pressure or target applied power was observed. The lowest adherences were associated with intermediate pressures and powers. The outstanding film to substrate adherence was mainly addressed to monophasic and nanometric film character (crystallite size was roughly 20 ± 10 nm) and to rather high continuity and homogeneity of films. ; El acero inoxidable UNS S31600 fue recubierto con películas de la aleación Ti6Al4V, por medio de la técnica pulverización catódica magnetrón rf. La superficie de los materiales obtenidos se sometió a ensayos de macroindentación, de acuerdo con el procedimiento VDI 3198, para caracterizar la adherencia película-sustrato. Se realizaron experimentos de depósito variando tanto la presión del gas al interior de la cámara de depósito como la potencia aplicada al blanco. La adherencia película-sustrato varío no monotónicamente con la presión y la potencia; la menor adherencia se observó para las presiones y las potencias intermedias. En términos generales se observó una excelente adherencia película-sustrato, la cual se atribuyó principalmente al carácter nanométrico de los cristalitos de las películas (diámetro promedio alrededor de 20 ± 10 nm), a su carácter monofásico y a su elevado grado de uniformidad tanto química como morfológica.
    • File Description:
      application/pdf; text/html
    • Relation:
      https://revistas.unal.edu.co/index.php/dyna/article/view/38019/pdf_24; https://revistas.unal.edu.co/index.php/dyna/article/view/38019/53993; García, C., Paucar, C. y Gaviria, J. Estudio de algunos parámetros que determinan la sintesis de hidroxiapatita por la ruta de precipitación. Dyna, 148, pp 9-15, 2006.; Copete, H., Lopez, M., Vargas, F., Echavarría, A. y Rios, T. Evaluación del comportamiento in vitro de recubrimientos de hidroxiapatita depositados mediante proyección térmica por combustión oxiacetilénica sobre un sustrato de Ti6Al4V. Dyna, 177, pp 101-107, 2013.; Anselme, K., Noel, B. and Hardouin, P. Human Osteoblast Adhesion on Titanium Alloy, Stainless Steel, Glass and Plastic Substrates with Same Surface Topography. J. Materials Science-Mater. Med., 10, pp815-819, 1999.; Balazic, M., Kopac, J., Jackson, J. M. and Ahmed, W. Titanium and Titanium Alloy Applications in Medicine. Int. J. of Nano and Biomaterials, 1, pp 3-34, 2007.; Dorozhkin, S.V. Bioceramics Based on Calcium Orthophosphates, Glass and Ceramics. 64, pp 442-447, 2007.; Niinomi, M. Mechanical Biocompatibilities of Titanium Alloys for Biomedical Applications. J. Mechanical Behaviour of Biomedical Materials, 1, pp 30-42, 2008.; Miura, K., Yamada, N., Hanada, S., Jung, T. and Itoi, E. The bone tissue compatibility of a new Ti-Nb-Sn alloy with a low Young's modulus. Acta Biomaterialia, 7, pp 2320-2326, 2011.; Yilmazer, H., Niinomi, M., Nakai, M. Cho, K. Hieda, J., Todaka, Y. and Miyazaki, T. Mechanical properties of a medical β-type titanium alloy with specific microstructural evolution through high-pressure torsion. Materials Science and Engineering C, 33, pp 2499–2507, 2013.; Lee, C., Chua, J., Chang, W., Lee, J., Jangc, J. and Liawd, P. Fatigue property improvements of Ti–6Al–4V by thin film coatings of metallic glass and TiN: a comparison study. Thin Solid Films, in press, corrected proof, disponible en linea (https://doi.org/10.1016/j.tsf.2013.08.027) 14 August 2013.; Zalnezhad, E., Baradaran, S., Bushroa, R. and Sarhan, A. Mechanical Property Enhancement of Ti-6Al-4V by Multilayer Thin Solid Film Ti/TiO2 Nanotubular Array Coating for Biomedical Application. Metallurgical and Materials Transactions A, 45A, pp 785-797, 2014.; De Souza, G., De Lima, G., Kuromoto, N., Soares, P., Lepienski, C., Foerster, C. and Mikowski, A. .Tribo-mechanical characterization of rough, porous and bioactive Ti anodic layers. Journal of the mechanical behavior of biomedical materials, 4, pp 796-806, 2011.; Erisir, E., Suadiye, E. and Gümüs, S. Microstructural characterization of wear of Arc-PVD Ti and Ti6Al4V coated austenitic stainless steels in Ringer's solution, Proceedings of 3rd International Conference of Engineering Against Failure (ICEAF III), pp. 421-427, 2013.; Zoestbergen, E. and De HOSSON, J. Crack Resistance of PVD Coatings: Influence of Surface Treatment Prior to Deposition, Surface Engineering, 18, pp 283-288, 2002.; Heinkea, W., Leylanda, A., Matthewsa, A., Bergb, G., Friedrichb, C. and Broszeitb, E. Evaluation of PVD nitride coatings, using impact, scratch and Rockwell-C adhesion tests, Thin Solid Films, 270, pp 431-438, 1995.; Ollendorf, H. and Schneider, D. A comparative study of adhesion test methods for hard coatings, Surface and Coatings Technology, 113, pp 86-102, 1999.; VDI - Verein Deutscher Ingenieure, Procedimiento 3198: Beschichten von Werkzeugen der Kaltmassivumformung; CVD- und PVD-Verfahren, Alemania, 1992.; Vidakisa, N. Antoniadis, A. and Bilalis N. The VDI 3198 indentation test evaluation of a reliable qualitative control for layered compounds, Journal of Materials Processing Technology, pp 143-144, 481-485, 2003.; https://revistas.unal.edu.co/index.php/dyna/article/view/38019
    • Rights:
      Derechos de autor 2014 DYNA ; https://creativecommons.org/licenses/by-nc-nd/4.0
    • الرقم المعرف:
      edsbas.A19F111F