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Highly Simple Deep Eutectic Solvent Extraction of Manganese in Vegetable Samples Prior to Its ICP-OES Analysis.

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  • المؤلفون: Bağda E;Bağda E; Altundağ H; Altundağ H; Soylak M; Soylak M
  • المصدر:
    Biological trace element research [Biol Trace Elem Res] 2017 Oct; Vol. 179 (2), pp. 334-339. Date of Electronic Publication: 2017 Feb 23.
  • نوع النشر :
    Journal Article
  • اللغة:
    English
  • معلومة اضافية
    • المصدر:
      Publisher: Humana Press Country of Publication: United States NLM ID: 7911509 Publication Model: Print-Electronic Cited Medium: Internet ISSN: 1559-0720 (Electronic) Linking ISSN: 01634984 NLM ISO Abbreviation: Biol Trace Elem Res Subsets: MEDLINE
    • بيانات النشر:
      Original Publication: [London, Clifton, N. J.] Humana Press.
    • الموضوع:
      Chemical Fractionation/*methods ; Food Analysis/*methods ; Manganese/*isolation & purification ; Vegetables/*chemistry; Choline/chemistry ; Citric Acid/chemistry ; Limit of Detection ; Manganese/analysis ; Oxalic Acid/chemistry ; Solvents/chemistry ; Spectrum Analysis/methods ; Temperature ; Time Factors
    • نبذة مختصرة :
      In the present work, simple and sensitive extraction methods for selective determination of manganese have been successfully developed. The methods were based on solubilization of manganese in deep eutectic solvent medium. Three deep eutectic solvents with choline chloride (vitamin B4) and tartaric/oxalic/citric acids have been prepared. Extraction parameters were optimized with using standard reference material (1573a tomato leaves). The quantitative recovery values were obtained with 1.25 g/L sample to deep eutectic solvent (DES) volume, at 95 °C for 2 h. The limit of detection was found as 0.50, 0.34, and 1.23 μg/L for DES/tartaric, DES/oxalic, and DES/citric acid, respectively. At optimum conditions, the analytical signal was linear for the range of 10-3000 μg/L for all studied DESs with the correlation coefficient >0.99. The extraction methods were applied to different real samples such as basil herb, spinach, dill, and cucumber barks. The known amount of manganese was spiked to samples, and good recovery results were obtained.
    • Contributed Indexing:
      Keywords: Deep eutectic solvent extraction; Manganese; Vegetable samples
    • الرقم المعرف:
      0 (Solvents)
      2968PHW8QP (Citric Acid)
      42Z2K6ZL8P (Manganese)
      9E7R5L6H31 (Oxalic Acid)
      N91BDP6H0X (Choline)
    • الموضوع:
      Date Created: 20170225 Date Completed: 20180711 Latest Revision: 20180711
    • الموضوع:
      20231215
    • الرقم المعرف:
      10.1007/s12011-017-0967-5
    • الرقم المعرف:
      28233088